Nuclear fuel technology. Controlled-potential coulometric assay of plutonium1 Scope This document describes an analytical method for the electrochemical assay of pure plutonium nitrate solutions of nuclear grade, with a total uncertainty not exceeding 0,2 % at the confidence level of 0,95 for a single determination (coverage factor, K = 2). The method is suitable for aqueous solutions containing more than 0,5 g L plutonium and test samples containing between 4 mg and 15 mg of plutonium. Application of this technique to

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